3,4-MethyleneDioxyPhenyl-2-Propanone

3,4-MethyleneDioxyPhenyl-2-Propanone (MDP2P) is a yellow chemical that has a melting point of 87-88 °C and a Boiling point range of 115-170 °C at around 30 mmhg. MDP2P can be synthesized by oxidation of MDP2Pol (3,4-MethyleneDioxyPhenyl-2-Propanol) using either sodium chlorite or sodium hypochlorite in hydrochloric acid and a byproduct is chlorine gas (if hydrochloric acid isn't used, then you will get the haloform reaction). MDP2P can also be synthesized by a grignard reaction of 3,4-MethyleneDioxyBenzyl magnesium chloride (formed from 3,4-Methylenedioxybenzyl chloride and magnesium turnings in diethyl ether) and acetonitrile followed by hydrochloric acid work-up. MDP2P can also be synthesized from wacker oxidation of safrole. Reaction of MDP2P with an ethanol solution of ethylamine and Aluminum Galinstan amalgam reduces the MDP2P-ethylimine intermediate into MDEA. 3,4-MethyleneDioxyPhenyl-2-Propanone is a yellow oily ketone. It is yellow green in the sunlight. MDP2P can also be synthesized by reacting sesamyl tosylate (SmOTs,3,4-Methylenedioxyphenyl tosylate) with ethyl acetoacetate and sodium ethoxide and Copper iodide catalyst and heat. 3,4-MethyleneDioxyPhenyl-2-Propanone is also called Sesamyl-2-Propanone (Se2P, Ses2P, Sm2P), Sesamylacetone, and Piperonyl Methyl Ketone.

I synthesized 3,4-MethyleneDioxyPhenyl-2-Propanone (MDP2P) by reacting 3,4-MethyleneDioxyBenzyl magnesium chloride and acetonitrile followed by hydrochloric acid work-up.

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